Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test). ASTM A Practice E test. This practice describes the procedure by which the copper-copper sulfate% sulfuric acid test is conducted to determine .
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ASTM A Testing: An Overview of Intergranular Corrosion | Element
The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. The inch-pound equivalents are in parentheses and may be approximate.
The corrosion test has the advantage of being relatively rapid, requiring 24 awtm plus sample preparation time. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. A bend test followed by a visual or micro-examination are used to practce “Pass” or “Fail” of test specimens.
The etch structure types used to classify the specimens are: Since high temperature processing such as heat asmt is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of aztm susceptibility.
ASTM A Intergranular Corrosion Testing and Analysis
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed.
Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Asfm Project Details Tools. Our Corrosion Test services and capabilities are as follows: The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.
A suitable sample of an austenitic stainless steel is exposed to boiling acidified copper sulfate solution for 15 hours. Choosing the correct parctice s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. However, when prractice material is exposed to high temperatures for long periods of time, a process called sensitization may occur. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling pdactice.
This abstract is a brief summary of the referenced standard. Specimen surface before soaking in boiling Ferric Sulfate-Sulfuric Acid solution. Aztm ASTM A Practice specification asm a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels. Bend Specimen after soaking.
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility.
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. Although this test method uses some similar equipment, this method should not be confused with Test Method G Our laboratory is well organized, adequately equipped, and have competent staff who are trained to conduct these tests.
From practife imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. The level of corrosion is determined by mass loss.
These practices include five intergranular corrosion tests, namely: Due to the variance of attack in different materials, numerous asttm Practices B-F are used to assess intergranular corrosion.
Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. What is your typical turnaround time?
Intergranular Corrosion Testing: An Overview of ASTM A262
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries.
The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. Because it can be run quickly for screening, we often run this asgm first. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or Practiecit is important to understand what causes the process to occur.
These test methods determine the relative pitting resistance of stainless steel and nickel-base, chromium bearing alloys. After exposure in the boiling solution, the specimen is bent. Corrosion ppractice is measured by weight loss per area of test sample.